Question Nepieciešama palīdzība 4mmc sintēzes posmā

[Kiteretsu_D]

Tātad es vispirms kolbā pievienoju 2b4mp, tad bezēnu, tad pievienoju metilamīnu 40 % un sāku maisīt ar megnetic maisītāju, tagad man nav siltuma avota, tāpēc cik ilgi man vajadzētu maisīt bez siltuma? Un kā es zinu, ka reakcija ir pabeigta? Sākumā šķidrums bija balts, tagad tas ir kļuvis zaļgans.

 

[Argento]

why did you use benzene instead of ethyl acetate or DCM?

 

[The-Hive]

Read this thread

 

[Osmosis Vanderwaal]

Its all a blur, but i seem to recall refluxing at under 105c for 2 hours or something. im not confident it will even react without the application of heat. Im old and all of the synths in my head turn into one massive synthesis of an end-game drug, and its hard to remimber which procedure goesvwith which synth, so i might be mistaken but i think you need at least enough energy to kick off the reaction

 

[Berlin777]

You can do cold synthesis and stir for 16h at room temperature