PMK Oil Synthesys From PMK (CAS 28578-16-7 Wax Form) Large Scale

[G.Patton]

This post is a good explanation, which was posted @btcboss2022 (thank you). I confirm, that it is a proven and working method.

 

[C14]

Hello master please you can tellme if the pmk ethyl.glycidate powder is soluble in ethanol? BecouseI read that 10mg/ml, that mean that i need 100 ml ethanol x 1 gram pmk ? I need know how many ml i need for 100 grams powder thanks

 

[G.Patton]

10 mg/ml = 1000mg/100ml or 1g/100ml

 

[ukises]

Hello Funciona.para el pmk ethyl powder???

 

[G.Patton]

MP of what?

 

[C14]

My pmk powder got ph 10 i think is sodium pmk glycidate, so i need use.only hcl? Thanks i wait your answer

 

[G.Patton]

What CAS your PMK powder has? This product has no pH due to it's not acid or base.

>>>i think is sodium pmk glycidate, so i need use.only hcl?
I have no any logic explanations why do you think so.

 

[Tippingpointover]

Hi, if I don’t have a reactor would this work?

1. Put 475 g of distilled h2o in a beaker and dissolve 25g of sodium bicarbonate
2. 70 g distilled h2o into a boiling flask
3. While stirring add 12 g sodium hydroxide
4. Bring mixture up to 60c
5. In a pot melt 50g of pmk wax
6. Add to the h20 and sodium hydroxide mix
7. Bring up to 80c slowly and reflux for an hour
8. Add 3.25g Hcl 37% slowly- reflux for one hour at 80c while stirring
9. After one hour- stop stirring and bring mixture down to 25c
10. Separate water layer from oil
11. Add oil layer back to boiling flask
12. Add h20 and sodium mix from step 1- stir for 2-3 min
13. Add 100g of dcm
14. Allow separation for 15 min
15. Distill dcm from solvent at 104f
16. Collect mdp-2-p

 

[C14]

Hello hcl only 3.25 grams??