Синтез на PMK масло от PMK (CAS 28578-16-7 восъчна форма) в голям мащаб

[Curiousonion]

Ами този метод е за pmk CAS 28578-16. Така че можете да го получите под формата на прах, след което той се превръща в масло, след като приключите с реакцията.
Но това изглежда изключително лесно, някой опитвал ли е това?

 

[C14]

It is bullshit from powder pmk dont work

 

[G.Patton]

Тази публикация е добро обяснение, което е публикувано от @btcboss2022 (благодаря). Потвърждавам, че това е доказан и работещ метод.

 

[C14]

Hello the pmk powder gkyciate got one special smell?? Maybe i.got fake pmk

 

[ukises]

Hello Funciona.para el pmk ethyl powder???

 

[C14]

Your methode Dont work for pmk powder

 

[G.Patton]

Hello, the method in this topic work for PMK methyl glycidate as well

 

[C14]

Methyl , but really for pmk ethyl powder dont work,thanks

 

[Jordan Belfort]

You mean that dark pmk powder with only desolved with ethanol/alcohol @C14

 

[G.Patton]

Are you sure that you have PMK ethyl glycidate?

 

[C14]

Really now not sure, i am cheking my pmk powder dont have any smell , i mean odor, it is neutro

 

[G.Patton]

It's not a test, check its melting point and compare with a literature data.

 

[realboss]

10. Add the H2O and sodium bicarbonate mixture, stirring 2-3 minutes.
11. Add 10 liters of DCM (from freezer preferably).
12. Let it get separated around 10-15 min.
13. Evaporate DCM from the bottom layer.

also in after dcm add step 12 any layer sepration heppen ?
@btcboss2022
and last qustion what is the purity of mdp2p

 

[G.Patton]

>also in after dcm add step 12 any layer sepration heppen ?
What do u mean? Try to read your question before to post and understand, Is it readable or has a sense?
>and last qustion what is the purity of mdp2p
@btcboss2022 will not answer cuz he's offline Aprill 22th 2024.
It isn't possible to answer this question.
The same as ask, will your soup be taste? Nobody know how are you prepare it, dude...

 

[realboss]

. Add 3.25kg of HCL 37% in small portions, once all added keep the mixture at 80 °C reflux during 1 h stirring.
hcl 37% water solution ?

 

[C14]

Hello for what use.the s bicarbonate, for clean or.for change ph?

 

[Jordan Belfort]

Both, and probably some NaCl will be formed if aquous HCL has been used, resulting in general better kinetics (if minor trace stays in the oil).

 

[G.Patton]

It's need to carry out alkaline hydrolysis of ester.