I was looking at a route with good yields, the scarecrow route, but in this route we only have the first part of the synthesis, which would be helional + dmso + hydroxylamine and sodium hydroxide as a base, after cooking for 90 minutes at 85 degrees we add 30% hydrogen peroxide, after that we...
Hi!
Attempts at the one-pot Helional to helionamide process, without successful results.
Issues seem to be the same some people encountered, so if you can give some hindsight it’d be greatly appreciated:
- 13,5g hidroxilamine are added to 175ml DMSO, heating and stirring until it’s dissolved...
The aim of this post is to summarize several months of research and testing. It would be great if everyone could share their results and their thoughts in order to perfect this synthesis route.
All the reagents I'll be using can probably be found in any hardware store, except for helional...
Introduction
Helional [CAS 1205-17-0] is rather interesting substance, which can serve as MDA precursor in the represented simple synthesis. In addition, it has opportunity to become a new MDMA precursor in case MDA conversion to MDMA. BB Forum team are working on this issue after recent China's...