Spôsoby výroby N-metylformamidu (NMF) ?

blackchip

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musím si vybrať medzi chloridom ortuťnatým alebo n-metylformamidom na syntézu mdma. nechcem žiadny odpad z ortuti, ale nmf je sledovaná chemikália, takže existuje spôsob, ako môžem vyrobiť nmf?
 

Montecristo

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Ak máte bezpečné miesto dodania, zaobstaral by som si ho z Číny, ako by ste PMK. Syntéza nie je jednoduchá ako potrebná kyselina mravčia.
 

G.Patton

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Dobrý deň. Na výrobu N-metylformamidu musíte nájsť metylamín, takže si myslím, že sa ho oplatí kúpiť.
 
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blackchip

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Kyselina mravčia sa dá ľahko vyrobiť z kyseliny šťaveľovej a glycerínu
 

daqwen

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Vďaka Bohu, že si ju môžem ľahko kúpiť v mojej krajine
 

Blammo

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You could just form methylammonium formate, and use instead. The leuckart works with alkylammonium formate salts. The temperature of the reaction is likely lower however.

Or get borohydride.

The leuckart is very low yielding, but simple and it scales well.
 
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