BMK Glycidate Sodium Salt Synthesis

[Arakava]

I added NAOH and stirred for 12 hrs at RT and 2 hrs at 60°c and let it cooled down. But it's still liquid. I think there is too much water in it. What should I do? Should I add hcl or first separate layers with toluene? Tnx

 

[G.Patton]

Added to what? How much? Your question is quite abstract.

 

[G.Patton]

It has to be heated to 80-90 °C and stired for 3 h.
Follow the method procedures:

 

[realboss]

If I replace Benzaldehyde with piperonal same amount end product is pmk ?
Is everything same every step just replace piperonal with Benzaldehyde
@G.Patton plz help boss

 

[G.Patton]

Hello, probably yes. We haven't carried out an experiment.

 

[realboss]

Thanks for kind reply

 

[realboss]

Can you make video on this topic boss
replace Benzaldehyde with piperonal same amount end product is pmk

 

[G.Patton]

Hi. I'm gonna post PMK glycidate synthesis from piperonal soon. We won't shot the video for this.

 

[MisterAnonymous]

@G.Patton Sodium ethylate 200 g (EtONa); can be replaced with Sodium Amide? How much Sodium Amide should i use ?

 

[G.Patton]

Hello, I don't know for sure. Probably, yes. If you want, you can try it in the same molar ratio.

 

[MisterAnonymous]

And you can replace Methyl 2-chloropropionate with Ethyl 2-chloropropionate right? Also in the same molar ratio because swim only haave access too Ethyl 2-chloropropionate